Synthesis and Phase Formation in Ba0.9Ca0.1Zr0.05M0.10Ti0.85O3 (M = Mn, Fe, Co) Ceramics with Controllable Magnetic and Optical Properties

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Resumo

Ceramic samples with perovskite structure of Ba0.9Ca0.1Zr0.05M0.10Ti0.85O3 (M = Mn, Fe, Co) were obtained by standard solid-phase synthesis methods. The processes of phase formation of samples by methods of X-ray phase analysis have been investigated, the parameters of unit cells have been determined. Magnetic and optical properties of the obtained samples were investigated by methods of magnetic susceptibility and diffuse reflection spectroscopy. It was found that the phase composition, as well as magnetic and optical properties depend on the nature of the introduced paramagnetic element.

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Sobre autores

A. Fedorova

Institute of Silicate Chemistry of Russian Academy of Sciences

Autor responsável pela correspondência
Email: avfiodorova@gmail.com
ORCID ID: 0000-0001-8242-5608
Rússia, Saint Petersburg

A. Selyutin

Saint Petersburg State University

Email: avfiodorova@gmail.com
ORCID ID: 0000-0002-5467-5658
Rússia, Saint Petersburg

N. Medzatyi

Institute of Silicate Chemistry of Russian Academy of Sciences

Email: avfiodorova@gmail.com
Rússia, Saint Petersburg

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2. Fig. 1. Diffractograms of Ba0.9Ca0.1Zr0.05Mn0.10Ti0.85O3 samples obtained by the standard solid-phase method under different charge calcination conditions.

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3. Fig. 2. Diffractograms of Ba0.9Ca0.1Zr0.05Fe0.10Ti0.85O3 samples obtained by the standard solid-phase method under different charge calcination conditions.

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4. Fig. 3. Diffractograms of Ba0.9Ca0.1Zr0.05Co0.10Ti0.85O3 samples obtained by the standard solid-phase method under different charge calcination conditions.

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5. Fig. 4. Temperature dependence of the experimental values of the effective magnetic moment (µef) for Ba0.9Ca0.1Zr0.05Fe0.10Ti0.85O3 (1), Ba0.9Ca0.1Zr0.05Mn0.10Ti0.85O3 (2), Ba0.9Ca0.1Zr0.05Co0.10Ti0.85O3 (3) samples.

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6. Fig. 5. Diffuse absorption spectra of Ba0.9Ca0.1Zr0.05Fe0.10Ti0.85O3 (1), Ba0.9Ca0.1Zr0.05Mn0.10Ti0.85O3 (2), Ba0.9Ca0.1Zr0.05Co0.10Ti0.85O3 (3) samples.

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7. Fig. 6. Diffuse reflectance spectra of samples: a - Ba0.9Ca0.1Zr0.05Fe0.10Ti0.85O3 (a); b - Ba0.9Ca0.1Zr0.05Mn0.10Ti0.85O3 (b); c - Ba0.9Ca0.1Zr0.05Co0.10Ti0.85O3 (c). E, eV.

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